HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → (8-Bromo-5-ethyl-2,3-dihydro-benzo[1,4]dioxin-6-yloxy)-acetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 8-Bromo-5-ethyl-2,3-dihydro-benzo[1,4]dioxin-6-ol | HCID 59598541 | — |
| Product | (8-Bromo-5-ethyl-2,3-dihydro-benzo[1,4]dioxin-6-yloxy)-acetonitrile | HCID 59598681 | — |
Reaction Steps
8-Bromo-5-ethyl-2,3-dihydro-benzo[1,4]dioxin-6-ol (3.182 g, 12.3 mmol), as described in the procedure of Step 6 of Example 21, was converted to cyanomethyl ether 8-Bromo-5-ethyl-2,3-dihydro-benzo[1,4]dioxin-6-yloxy)-acetonitrile (2.30 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858632B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-e495a67ec68b434886609b1c07761cd3 |
| Source note | uspto-grants-2010_12 |