HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenylacetic Acid → N-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-phenylacetohydrazide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenylacetic Acid | HCID 999 | — |
| Edukt | N'-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-cyclohexylacetohydrazide | HCID 57979752 | — |
| Produkt | N-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-phenylacetohydrazide | HCID 68688765 | 47% |
Reaktionsschritte
The title compound (42 mg, 47%) as a white foam was prepared from 2-phenylacetic acid (41 mg, 0.3 mmol) and 1-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3)hydrazine (66 mg, 0.2 mmol) according to the procedures described for N′-(6-(2-chlorophenyl)-5-(4-chlorophenyl)pyridazin-3-yl)-2-cyclohexylacetohydrazide (Example 7A). HPLC/MS (method A): retention time=3.30 min, (M+H)+=449.2.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07858639B2 |
| Quelldatensatz | uspto-grants-2010_12 |
| ORD ID | ord-5f095c48918c4c99b641e212c050f4f3 |
| Quellennotiz | uspto-grants-2010_12 |