4-Chlorophenylboronic acid → HCID 18444589, compound

HRID 2266824Notes

Reaction equation

HRID 2266824 reaction equation
C[O:2][C:3]([C:5]1[O:6][C:7](C)=[C:8]([CH2:10][O:11][C:12]2[CH:17]=[CH:16][C:15](I)=[CH:14][CH:13]=2)[CH:9]=1)=[O:4].Cl[C:21]1[CH:26]=[CH:25][C:24](B(O)O)=[CH:23][CH:22]=1>>[C:15]1([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[CH:14]=[CH:13][C:12]([O:11][CH2:10][C:8]2[CH:9]=[C:5]([C:3]([OH:2])=[O:4])[O:6][CH:7]=2)=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 742994-Chlorophenylboronic acidHCID 588241574-(4-Iodo-phenoxymethyl)-5-methyl-furan-2-carboxylic acid methyl ester

Product 1

HCID 18444589HCID 18444589, compound

Procedure

Compound (77) was prepared from compound (20) and (4-chloro-phenyl)-boronic acid by adapting the procedure of Example 5(b). LC/MS System B; Rt=1.93 mins, m/z (ES−)=341 and 343 (M−H for C19H15ClO4).

Sources & evidence

ORD record
ord-bf8598bddf1044ec8ad703702a625bfe
Source dataset
uspto-grants-2010_12
Patent number
US07858644B2

Reaction notes

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