HCID 58945830, compound → HCID 58945846, compound

HRID 2267133Notes

Reaction equation

HRID 2267133 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[CH:12]=[C:11]([C:13]2[CH2:14][CH2:15][N:16]([C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])[CH2:17][CH:18]=2)[N:10]=[N:9]1.[C:26](C1CCN(C(OC(C)(C)C)=O)CC=1)#CC>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:8]1[C:12]([CH3:26])=[C:11]([C:13]2[CH2:14][CH2:15][N:16]([C:19]([O:21][C:22]([CH3:25])([CH3:24])[CH3:23])=[O:20])[CH2:17][CH:18]=2)[N:10]=[N:9]1

Participants

3

Reactant 2

HCID 58945830HCID 58945830, compoundHCID 68431041HCID 68431041, compound

Product 1

HCID 58945846HCID 58945846, compound

Procedure

The same operation as in Example 7 was carried out using the azide compound prepared in Example 1 and tert-butyl 4-(1-propynyl)-1,2,3,6-tetrahydropyridine-1-carboxylate prepared in 3) of Example 7 to give the title compound as a white solid.

Workup

  1. customprepared in 3) of Example 7

Sources & evidence

ORD record
ord-ac3091885c4e43719b916dce2d0435d1
Source dataset
uspto-grants-2010_12
Patent number
US07858800B2

Reaction notes

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