TIBA isododecane → 2,3,5-Triiodobenzoic acid

Participants

Reaction Steps

8.1 mL of TIBA/isododecane solution (110 g/L) were mixed with 1.9 mL of MAO/toluene solution to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 30 minutes at room temperature. Then, 25 mg of C2 were added to give a clear solution, which was diluted with 4.4 mL of toluene to reach a concentration of 100 gTOT/L and 1.74 gmetallocene/L.

Provenance & Evidence