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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2267229Generated: October 30, 2026

Ethanol → HCID 57807684, compound

https://huagongshe.com/reaction/2267229

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 86650919HCID 86650919—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
ProductHCID 57807684HCID 57807684—

Reaction Steps

A suspension of 2.15 g (5.52 mmol) 1-benzyl-2-ethyl(S)-4-(1-methyl-piperidin-4-yl)-piperazine-1,2-dicarboxylate and 100 mg 10% Pd/C in 50 mL EtOH was hydrogenated for 2 h at 50° C. and 3447 hPa hydrogen pressure. The catalyst was filtered off and the filtrate was evaporated to dryness. The product was reacted further without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07858622B2
Source datasetuspto-grants-2010_12
ORD IDord-de75538a19d849e78ec75d411a73c71b
Source noteuspto-grants-2010_12