HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 57807684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 86650919 | HCID 86650919 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 57807684 | HCID 57807684 | — |
Reaction Steps
A suspension of 2.15 g (5.52 mmol) 1-benzyl-2-ethyl(S)-4-(1-methyl-piperidin-4-yl)-piperazine-1,2-dicarboxylate and 100 mg 10% Pd/C in 50 mL EtOH was hydrogenated for 2 h at 50° C. and 3447 hPa hydrogen pressure. The catalyst was filtered off and the filtrate was evaporated to dryness. The product was reacted further without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858622B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-de75538a19d849e78ec75d411a73c71b |
| Source note | uspto-grants-2010_12 |