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HRID226724

反应详情

EQUATION

反应方程式

HRID 226724 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccc2c(c1)CCO2
HCID2735367

1-(2,3-Dihydro-1-benzofuran-5-yl)methanamine

C9H11NO

结构：Fc1cnc(Cl)nc1Nc1ccc2c(c1)OCCO2
HCID22060362

未命名化合物

PRODUCTS

生成物

1
结构：Fc1cnc(NCc2ccc3c(c2)CCO3)nc1Nc1ccc2c(c1)OCCO2
HCID22061054

未命名化合物

PROCEDURE

实验过程

In like manner to the preparation of N4-(3-aminophenyl)-N2-[2-(methoxycarbonyl)-benzofurane-5-yl]-5-fluoro-2,4-pyrimidinediamine, 2-chloro-N4-(3,4-ethylenedioxyphenyl)-5-fluoro-4-pyrimidineamine and 2,3-dihydrobenzo[b]furan-5-ylmethylamine were reacted to give N2-[2,3-dihydrobenzo[b]furan-5-ylmethyl]-N4-(3,4-ethylenedioxyphenyl)-5-fluoro-2,4-pyrimidinediamine. LCMS: ret. time: 21.43 min.; purity: 97.5%; MS (m/e): 395.05 (MH+).

WORKUP

后处理

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