HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 11512497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 86616132 | HCID 86616132 | — |
| Product | HCID 11512497 | HCID 11512497 | 30% |
Reaction Steps
Following the general procedure of example (99), 3-(1-{[3-(dimethylamino)propyl]sulfonyl}-4-piperidinyl)-5-(4-formylphenyl)-1H-indole-7-carboxamide (50 mg, 0.1 mmol), morpholine (9 mg, 0.1 mmol) and NaBH(OAc)3 (64 mg, 0.3 mmol) were reacted to give the title compound (15 mg, 30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858796B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-b94f8b88411a431dbd82f3a5330d48c4 |
| Source note | uspto-grants-2010_12 |