HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 59003283, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-chloro-1,3-dimethyl-1H-pyrazole-4-sulfonyl chloride | HCID 2777126 | — |
| Reactant | 5-Phenyl-3-(4-piperidinyl)-1H-indole-7-carboxamide | HCID 11427162 | — |
| Product | HCID 59003283 | HCID 59003283 | — |
Reaction Steps
Following the general procedure in example 267, 5-(phenyl)-3-(4-piperidinyl)-1H-indole-7-carboxamide (32 mg, 0.1 mmol), 5-chloro-1,3-dimethyl-1H-pyrazole-4-sulfonyl chloride (34.5 mg, 0.15 mmol) and triethylamine (0.06 mL, 0.3 mmol) were reacted to form the desired product which was purified by Gilson HPLC (CH3CN/Water, 0.1% TFA) (22 mg, 43%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07858796B2 |
| Source dataset | uspto-grants-2010_12 |
| ORD ID | ord-a9da6a8dce7548969732c6f46a8da048 |
| Source note | uspto-grants-2010_12 |