3-Nitrophthalic acid → 1,2,3,4-Tetramethyl imidazolinium.3-nitrophthalate

HRID 2267954Notes

Reaction equation

HRID 2267954 reaction equation
[N+:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:6]([C:7]([OH:9])=[O:8])[C:5]=1[C:13]([OH:15])=[O:14])([O-:3])=[O:2].COC(=O)[O-].[CH3:21][NH+:22]1[CH2:26][CH:25]([CH3:27])[N:24]([CH3:28])[CH:23]1[CH3:29]>>[CH3:21][NH+:22]1[CH2:26][CH:25]([CH3:27])[N:24]([CH3:28])[CH:23]1[CH3:29].[N+:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:6]([C:7]([O-:9])=[O:8])[C:5]=1[C:13]([O-:15])=[O:14])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 690433-Nitrophthalic acidHCID 675213621,2,3,4-Tetramethylimidazolinium methyl carbonate

Product 1

HCID 866256591,2,3,4-Tetramethyl imidazolinium.3-nitrophthalate

Procedure

Next, 3-nitrophthalic acid (0.1 mol) was added into a 1,2,3,4-tetramethyl imidazolinium methyl carbonate salt (0.1 mol) solution to induce a salt exchange reaction, thereby obtaining a 1,2,3,4-tetramethyl imidazolinium•3-nitrophthalate solution.

Workup

  1. customa salt exchange reaction

Sources & evidence

ORD record
ord-45dd2c88a0f34188b6520fbaeece2992
Source dataset
uspto-grants-2010_12
Patent number
US07859828B2

Reaction notes

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