HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11011614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18432352 | HCID 18432352 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 11011614 | HCID 11011614 | — |
Reaction Steps
20.0 g (0.075 mol) of 4,4,8-trimethyl-1,1-dioxothiochroman-7-carboxylic acid were dissolved in 200 ml of toluene and three drops of dimethylformamide and 10.7 g (0.09 mol) of thionyl chloride were added. After three hours of heating under reflux, the solvent was removed and the colorless oil that remained (yield 21.3 g) was directly used further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326333B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-5b8aac480a98486b93efb9831c163510 |
| Source note | uspto-grants-2001_12 |