HCID 12073915, compound → HCID 12073916, compound

Participants

Reaction Conditions

Reaction Steps

2.77 g (9 mmol) of 1-(3,5-di-tert.-butyl-2-butyloxyphenyl)ethanol was dissolved in 120 ml of toluene that had been treated with 14 g of manganese(IV)oxide. This was well stirred at 75° C. for 5 hr. This was cooled and filtered through celite. Solvent was removed to give 2.27 g of 1-(3,5-di-tert.-butyl-2-butyloxyphenyl)ethanone. 1H NMR (CDCl3) δ 7.38 (dd,4H,aromatics), 2.62 (s,3H, CH3C—), 3.72 (t, 2H, —OCH2—).

Provenance & Evidence