HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → Diisopropylethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Levulinic Acid | HCID 11579 | — |
| Reactant | Diisopropylcarbodiimide | HCID 12734 | — |
| Product | Diisopropylethylamine | HCID 81531 | — |
Reaction Steps
addition of activated levulinic acid (activated as the symmetric anhydride with 0.5 equivalents of DIC in DCM for 5-10 min)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326468B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-58b6aac9bc1741729dd9a2325fc906f9 |
| Source note | uspto-grants-2001_12 |