HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl 3-hydroxybenzoate → Allyl 3-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyloxy]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl 3-hydroxybenzoate | HCID 13137382 | — |
| Reactant | 3-(5,6,7,8-Tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride | HCID 73431556 | — |
| Product | Allyl 3-[3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyloxy]benzoate | HCID 70213311 | — |
Reaction Steps
In a similar manner to that of Example 1(d), by reaction of 2.8 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)acryloyl chloride with 1.8 g (10 mmol) of allyl 3-hydroxybenzoate, 2.6 g (62%) of the expected allyl ester are obtained in the form of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326510B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-fc01bcbf7e8841cfbfa13fc71c40a8b8 |
| Source note | uspto-grants-2001_12 |