Thionyl Chloride → HCID 73431553, compound

HRID 2268220Notes

Reaction equation

HRID 2268220 reaction equation
[CH3:1][C:2]1([CH3:20])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6]([C:14]([CH3:19])=[CH:15][C:16](O)=[O:17])[CH:5]=[CH:4][C:3]1=2.S(Cl)([Cl:23])=O>>[CH3:1][C:2]1([CH3:20])[CH2:11][CH2:10][C:9]([CH3:13])([CH3:12])[C:8]2[CH:7]=[C:6]([C:14]([CH3:19])=[CH:15][C:16]([Cl:23])=[O:17])[CH:5]=[CH:4][C:3]1=2

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 54560254HCID 54560254, compound

Product 1

HCID 73431553HCID 73431553, compound

Procedure

In a similar manner to that of Example 1(c), by reaction of 2.7 g (10 mmol) of 3-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-butenoic acid with 800 μl of thionyl chloride, 2.9 g (100%) of the expected acid chloride are obtained, which product will be used subsequently in the synthesis without further purification.

Workup

  1. customare obtained
  2. customwhich product will be used subsequently in the synthesis without further purification

Sources & evidence

ORD record
ord-d775812af88345a798187bb47332dd8c
Source dataset
uspto-grants-2001_12
Patent number
US06326510B1

Reaction notes

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