HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Sulfite → (4-Cyanophenyl)methanesulfonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Product | (4-Cyanophenyl)methanesulfonyl chloride | HCID 15480555 | — |
Reaction Steps
4-Bromomethylbenzonitrile was reacted with sodium sulphite followed by phosphorus pentachloride to give 4-cyanobenzylsulphonyl chloride which was reacted with pentylamine in a similar manner to N14 to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326500B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-63e51071a52e48dfa507a4d87147ca5f |
| Source note | uspto-grants-2001_12 |