HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Xylenethiol → methyl N-{1-methyl-1-[4-(3,4-xylylthiomethyl)phenyl]ethyl}carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Xylenethiol | HCID 87799 | — |
| Reactant | methyl N-(1-(4-bromomethylphenyl)-1-methylethyl]carbamate | HCID 18349698 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | methyl N-{1-methyl-1-[4-(3,4-xylylthiomethyl)phenyl]ethyl}carbamate | HCID 18349783 | — |
Reaction Steps
A solution of 3,4-dimethylbenzenethiol (9.24 g) in DMF (30 ml) reacted with a solution of methyl N-[1-(4-bromomethylphenyl)-1-methylethyl]carbamate (19.15 g) in DMF (100 ml) by Method 6a) to give methyl N-{1-methyl-1-[4-(3,4-xylylthiomethyl)phenyl]ethyl}carbamate as a sticky solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06326500B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-f40cefd7fe1f4f63b0cf8407048740df |
| Source note | uspto-grants-2001_12 |