Acetic Acid → HCID 10208793, compound

Participants

Reaction Steps

The title compound was prepared by a similar method to example 6 from (2R,3R,4S,5R)-2-{2-(aminomethyl)-6-[(2,2-diphenylethyl)amino]-9H-purin-9-yl}-5-(methoxymethyl)tetrahydro-3,4-furandiol (example 1) (100 mg, 0.20 mmol), acetone (12 mg, 0.21 mmol), sodium triacetoxyborohydride (70 mg, 0.33 mmol) and acetic acid (0.14 ml, 0.25 mmol) to afford the title compound (63 mg). MS: 533 (MH+).

Provenance & Evidence