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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2268659Generated: October 31, 2026

Trifluoroacetic acid → HCID 18349208, compound

https://huagongshe.com/reaction/2268659

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 54569549HCID 54569549—
SolventDichloromethaneHCID 6344—
ProductHCID 18349208HCID 18349208—

Reaction Steps

A solution of (2-{3-chloro-5-[(2-cyano-ethyl)-cyclopropylmethyl-carbamoyl]-phenoxy}-ethyl)-pyridin-4-yl-carbamic acid tert-butyl ester (0.07 g) in a mixture of dichloromethane (5 ml) and trifluoroacetic acid (2 ml) was stored at room temperature for 18 h and then concentrated under reduced pressure to give the title compound as a light brown oil (0.071 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06326386B1
Source datasetuspto-grants-2001_12
ORD IDord-414dbf126a1c406bb722e62c7adc172b
Source noteuspto-grants-2001_12