化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-Benzyloxy-4-methoxybenzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-Benzyloxy-p-anisic acid | HCID 94057 | — |
| 生成物 | 3-Benzyloxy-4-methoxybenzoyl chloride | HCID 10967795 | 98% |
反応手順
A solution of 3-benzyloxy-4-methoxy-benzoic acid (35.86 g, 0.139 mole), prepared as described in example 53, in thionyl chloride (150 ml) was refluxed for 2 hours under N2, evaporated to dryness and taken up twice in toluene (100 ml) to give 35.01 g of the title compound (yield: 98%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06329370B1 |
| 出典データセット | uspto-grants-2001_12 |
| ORD ID | ord-d29d08aefc924e338d9e8ee0e76787a8 |
| 出典メモ | uspto-grants-2001_12 |