Cyclohexanemethylamine → HCID 9948519, compound

Participants

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine (EXAMPLE 1) was reacted with aminomethylcyclohexane according to the procedure described in EXAMPLE 11, Step C to afford the title compound. Mass Spectrum (ESI): 308.3 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.64 (s, 1H); 8.39 (br s, 1H); 8.23 (br s, 1H); 7.87 (m, 1H); 7.41 (m, 2H); 6.78 (d, J=5.5 Hz, 1H); 5.50 (br s, 1H); 3.39 (t, J=6.3 Hz, 2H) 1.70-1.93 (m, 6H); 1.18-1.38 (m, 3H); 1.02-1.12 (m, 2H).

Provenance & Evidence