(S)-(+)-1-Cyclohexylethylamine → HCID 45486772, compound

Participants

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine (EXAMPLE 1) was reacted with (S)-1-cyclohexylethylamine according to the procedure described in EXAMPLE 11, Step C to afford the title compound. Mass Spectrum (ESI): 322.3 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.63 (s, 1H); 8.30 (br s, 1H); 8.23 (br, s, 1H); 7.88 (d, J=7.3 Hz, 1H); 7.43 (m, 2H); 6.80 (d, J=5.2 Hz, 1H); 4.10 (m, 1H); 1.69-1.91 (m, 4H); 1.10-1.35 (m, 10H).

Provenance & Evidence