HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178458945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 6-Amino-9-benzyl-8-methoxy-2-propoxypurine | HCID 10881541 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178458945 | HCID 178458945 | 83% |
Reaction Steps
6-Amino-9-benzyl-8-methoxy-2-propoxypurine (75 mg, 0.24 mmol) in concentrated hydrochloric acid (15 ml) was stirred for 3 hours at room temperature. The reaction mixture was made basic with 28% aqueous ammonia, and the resulting crystals were filtered and washed with water to give the subject compound (59 mg, yield 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-a51b6313541d4a3194878f1efa76d072 |
| Source note | uspto-grants-2001_12 |