HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178447010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 6-Amino-9-benzyl-8-methoxy-2-pentoxypurine | HCID 11024299 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 178447010 | HCID 178447010 | 86.2% |
Reaction Steps
6-Amino-9-benzyl-8-methoxy-2-pentoxypurine (40 mg, 0.117 mmol) in concentrated hydrochloric acid (20 ml) was stirred for 12 hours at room temperature. The reaction mixture was made basic with 28% aqueous ammonia. The resulting crystals were filtered and washed with water to give the subject compound (33 mg, yield 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329381B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-3dd530392f6c4f4c94c6f62c18bf6585 |
| Source note | uspto-grants-2001_12 |