HuagongsheHuagongshe Chemistry Print Report · For research reference only
(-)-Mandelic acid → HCID 131723012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (-)-Mandelic acid | HCID 11914 | — |
| Reactant | HCID 69712392 | HCID 69712392 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 131723012 | HCID 131723012 | 66% |
Reaction Steps
To a solution of Compound 36 (179 mg, 0.50 mmol) in ethanol (3 ml) was added (R)-(−)-mandelic acid (75.4 mg, 0.50 mmol) at room temperature. After the solvent was evaporated in vacuo, the residue was recrystallized from ethanol-diethyl ether to give Compound 37 (168 mg, 66%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329396B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-2ccb52cd1a2f416193f37842e5a7075b |
| Source note | uspto-grants-2001_12 |