Sodium borohydride → HCID 70189772, compound

Participants

Reaction Steps

In a similar manner to that described in Example (15b), N-[(3-nitrophenyl)-2-thienylmethyl]-N-[(S)-1-phenylethyl]amine (4.56 g) [prepared as described in step (a) above], nickel chloride hexahydrate (6.42 g) and sodium borohydride (2.04 g) were reacted and purified, to afford isomer A of the title compound (936 mg) as a pale yellow oil and isomer B of the title compound (380 mg) as a pale yellow oil.

Provenance & Evidence