HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334117 | HCID 18334117 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18334098 | HCID 18334098 | 22.4% |
Reaction Steps
In a similar manner to that described in Example (1b), a solution of N-[2-(1H-indol-3-yl)ethyl]-N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]amine (2.33 g) [prepared as described in step (a) above] in ethanol (50 ml), nickel chloride hexahydrate (2.76 g) and sodium borohydride (878 mg) were reacted, to afford the title compound (484 mg) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-13fb10f66b844001a9ce173cf0c04a6e |
| Source note | uspto-grants-2001_12 |