Sodium borohydride → HCID 18334211, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (59b), 3.30 g of N-[(4-fluorophenyl)-(3-nitrophenyl)methyl]-N-[1-(3,4,5-trifluorophenyl)ethyl]amine [prepared as described in step (a) above], 3.96 g of nickel chloride hexahydrate and 1.25 g of sodium borohydride were reacted, to obtain 1.25 g of isomer A and 975 mg of isomer B of the title compound as pale yellow oils, respectively.

Provenance & Evidence