Sodium borohydride → HCID 18334100, compound

Participants

Reaction Steps

Following a similar procedure to that described in Example (1b), 700 mg of isomer A of N-[1-(3,4-difluorophenyl)ethyl]-N-[(4-fluorophenyl)-(2-methoxy-5 nitrophenyl)methyl]amine [prepared as described in step (a) above], 800 mg of nickel chloride hexahydrate and 258 mg of sodium borohydride were reacted, to obtain 532 mg of isomer A of the title compound as a pale yellow oil.

Provenance & Evidence