(R)-1-(4-Methoxyphenyl)ethylamine → HCID 70190086, compound

HRID 2269478Notes

Reaction equation

HRID 2269478 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)=O)[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[CH3:20][O:21][C:22]1[CH:27]=[CH:26][C:25]([C@H:28]([NH2:30])[CH3:29])=[CH:24][CH:23]=1>>[CH3:20][O:21][C:22]1[CH:27]=[CH:26][C:25]([C@H:28]([NH:30][CH:10]([C:12]2[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=2)[C:6]2[CH:7]=[CH:8][CH:9]=[C:4]([N+:1]([O-:3])=[O:2])[CH:5]=2)[CH3:29])=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 641449(R)-1-(4-Methoxyphenyl)ethylamineHCID 794540(4-Methoxyphenyl)(3-nitrophenyl)methanone

Product 1

HCID 70190086HCID 70190086, compound

Procedure

Following a similar procedure to that described in Example (1a), 6.00 g of 4-methoxyphenyl 3-nitrophenyl ketone and 5.32 g of (R)-1-(4-methoxyphenyl)ethylamine were reacted, to obtain 8.83 of the title compound as a pale yellow oil.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-2a5ea23adbff407d863e80d0072f6dda
Source dataset
uspto-grants-2001_12
Patent number
US06329405B1

Reaction notes

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