Sodium borohydride → HCID 70189793, compound

Participants

Reaction Steps

Following a similar procedure to that described in Example (1b), 1.63 g of isomer B of N-[(R)-1-(3-fluorophenyl)ethyl]-N-[(4-fluorophenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 2.11 g of nickel chloride hexahydrate, 6.74 g of sodium borohydride and 20 ml of methanol were reacted, to obtain 1.45 g of isomer B of the title compound as a colorless oil.

Provenance & Evidence