Sodium borohydride → HCID 18334152, compound

Participants

Reaction Steps

Following a similar procedure to that described in Example (1b), 920 mg of isomer A of N-[1-(3,4-difluorophenyl)ethyl]-N-[(2,4-dimethoxyphenyl)-(3-nitrophenyl)methyl]amine [prepared as described in step (a) above], 1.02 g of nickel chloride hexahydrate, 325 mg of sodium borohydride and 50 ml of methanol were reacted, to obtain 543 mg of isomerci A of the title compound as a colorless oil.

Provenance & Evidence