HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334139 | HCID 18334139 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 18334251 | HCID 18334251 | 91.3% |
Reaction Steps
Following a similar procedure to that described in Example (1b), 3.34 g of N-[(4-methoxyphenyl)-(3-nitrophenyl)methyl]-N-[1-(3,4,5-trifluorophenyl)ethyl]amine [prepared as described in step (a) above], 3.81 g of nickel chloride hexahydrate and 1.22 g of sodium borohydride were reacted, to obtain 2.83 g of the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-e17b621c3afa4baf80a8bf7d1fbe8ef6 |
| Source note | uspto-grants-2001_12 |