Sodium borohydride → HCID 18334264, compound

Participants

Reaction Steps

Following a similar reaction, separation and purification procedure to that described in Example (59b), 2.71 g of N-[(4-chlorophenyl)-(3-nitrophenyl)methyl]-N-[1-(3,4,5-trifluorophenyl)ethyl]amine [prepared as described in step (a) above], 3.06 g of nickel chloride hexahydrate and 973 mg of sodium borohydride were reacted, to obtain 946 mg of isomer A and 691 mg of isomer B of the title compound as a colorless oil and white solid, respectively.

Provenance & Evidence