HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 18334183, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 18334196 | HCID 18334196 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 18334183 | HCID 18334183 | — |
Reaction Steps
Following a similar reaction, separation and purification procedure to that described in Example (59b), 7.76 g of N-[1-(3,4-difluorophenyl)ethyl]-N-[(3-nitrophenyl)-(p-tolyl)methyl]amine [prepared as described in step (a) above], 9.65 g of nickel chloride hexahydrate and 3.07 g of sodium borohydride were reacted, to obtain 1.67 g of isomer A and 2.37 g of isomer B of the title compound, each as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-d4b65351ae84479699291b5243515ebe |
| Source note | uspto-grants-2001_12 |