HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 70189745, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 70189147 | HCID 70189147 | — |
| Catalyst | Dichloronickel;hexahydrate | HCID 11791229 | — |
| Product | HCID 70189745 | HCID 70189745 | — |
Reaction Steps
Following a procedure similar to that described in Example (1b), 750 mg of isomer A of N-[(4-chlorophenyl)-(3-nitrophenyl)methyl]-N-[(R)-1-phenylethyl]amine [prepared as described in step (a) above], 972 mg of nickel chloride hexahydrate and 309 mg of sodium borohydride were reacted and purified, to obtain 640 mg of isomer A of the title compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329405B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-6e8a697f39364200affbbd28a96a7a1f |
| Source note | uspto-grants-2001_12 |