HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Propanol → 2,4-Dichlorobenzoyl Cyanide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Propanol | HCID 1031 | — |
| Reactant | HCID 178511374 | HCID 178511374 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2,4-Dichlorobenzoyl Cyanide | HCID 9834232 | — |
| Product | 6-(2,4-Dichlorophenyl)-1,2,4-triazine-3,5-diamine | HCID 18347897 | — |
Reaction Steps
The title compound was prepared as in Example 2(a) from 2,4-dichlorobenzoyl cyanide amidinohydrazone obtained in Example 3. The solvent for ring closure was a mixture of 1-propanol and dimethylsulfoxide (5:1). Total yield (from 2,4-dichlorobenzoyl cyanide): 55%; m.p. 220-222° C. (uncorrected).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329521B2 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-91a562f30f3a4a90bfbf3904bf4c121a |
| Source note | uspto-grants-2001_12 |