HCID 20713095, compound → HCID 18348124, compound

HRID 2269831Notes

Reaction equation

HRID 2269831 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:45]=[CH:46][C:47]=1[Cl:48])[CH2:5][CH2:6][NH:7][C:8](=[O:44])[CH:9]([NH:23][C:24](=[O:43])[C@@H:25]([S:33]CC1C=CC(OC)=CC=1)[CH2:26][C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)[C:10]([NH:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][C:18]([Cl:21])=[C:17]([Cl:22])[CH:16]=1)=[O:11]>C(Cl)(Cl)(Cl)Cl>[Cl:1][C:2]1[CH:3]=[C:4]([CH:45]=[CH:46][C:47]=1[Cl:48])[CH2:5][CH2:6][NH:7][C:8](=[O:44])[CH:9]([NH:23][C:24](=[O:43])[CH:25]([SH:33])[CH2:26][C:27]1[CH:28]=[CH:29][CH:30]=[CH:31][CH:32]=1)[C:10]([NH:12][CH2:13][CH2:14][C:15]1[CH:20]=[CH:19][C:18]([Cl:21])=[C:17]([Cl:22])[CH:16]=1)=[O:11]

Participants

3

Reactant 1

HCID 20713095HCID 20713095, compound

Product 1

HCID 18348124HCID 18348124, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

Prepare by the method of Example 15.2 using N,N′-di-(3,4-dichlorophenethyl)-2-((S)-2-(p-methoxybenzylmercapto)-3-phenylpropionylamino)malonamide (0.166 g, 0.222 mmol). Coevaporation with carbon tetrachloride gives the title compound.

Sources & evidence

ORD record
ord-06d9152747754bd8b33095b12cf36e13
Source dataset
uspto-grants-2001_12
Patent number
US06329550B1

Reaction notes

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