HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 15542875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 18333268 | HCID 18333268 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15542875 | HCID 15542875 | — |
Reaction Steps
Combine 1-(3,4,5-trimethoxy-benzoyl)-3-[2-[4-[1-(1-benzyl-imidazol-2-ylmethyl)-1H-benzoimidazole-2-carbonyl]-piperidin-1-yl]-ethyl]-3-phenyl-pyrrolidine (5 mmol) and 10% palladium-on-carbon (1.5 g) in methanol (50 mL). Add anhydrous ammonium formate (25 mmol). Heat to reflux. After 18 hours, filter, rinse with dichloromethane, and evaporate the filtrate in vacuo to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06329392B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-930bad214bd94db68e30d6c7f0eda28c |
| Source note | uspto-grants-2001_12 |