HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22632884, compound → HCID 9820196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22632884 | HCID 22632884 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 9820196 | HCID 9820196 | 77.3% |
Reaction Steps
Using the General Method 6A, the reaction of 10% Pd/C (0.027 g) with 1-(4-fluorophenyl)-6-fluoro-3-benzyloxy-7-pyrrolidin-1-yl-1H-quinazoline-2,4-dione (Example L-1, 0.08 g, 0.18 mmol) afforded 0.05 g of the title compound as a solid, mp 183-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331538B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-d1f88ea64cb24cc99b3d5fbf1ea71311 |
| Source note | uspto-grants-2001_12 |