HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22632929, compound → HCID 9887217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22632929 | HCID 22632929 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 9887217 | HCID 9887217 | 92.8% |
Reaction Steps
Using the General Method 6A, the reaction of 10% Pd/C (0.057 g) with 1-(4-methoxyphenyl)-6-fluoro-3-benzyloxy-7-(4-methylpiperazin-1-yl)-1H-quinazoline-2,4-dione (Example P-1, 0.17 g, 0.35 mmol) afforded 0.13 g of the title compound as a solid, mp 195-196° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331538B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-0168e9bdbd5b4bf78e9102a8a7d5d0c3 |
| Source note | uspto-grants-2001_12 |