HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 59071619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 22714957 | HCID 22714957 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59071619 | HCID 59071619 | 66.2% |
Reaction Steps
A suspension of 174 mg (0.4 mmol) of Compound 26, 56 mg (0.8 mmol) of hydroxylamine hydrochloride and 66 mg (0.8 mmol) of sodium acetate in 20 ml of methanol was refluxed for 17 hours. Post-treatment and purification were conducted in a similar manner as in Example 20, whereby 119 mg of the title compound were obtained (yield: 66%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331623B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-60851f5233f6452cb513402096563395 |
| Source note | uspto-grants-2001_12 |