HCID 18331414, compound → HCID 18331452, compound

HRID 2270550Notes

Reaction equation

HRID 2270550 reaction equation
[C:1]([O:5][C:6]([NH:8][CH2:9][C:10]1[CH:11]=[C:12]([NH:16][C:17]2[C:22]([CH2:23][OH:24])=[CH:21][CH:20]=[C:19]([O:25][CH3:26])[N:18]=2)[CH:13]=[CH:14][CH:15]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]>[O-2].[O-2].[O-2].[O-2].[Mn+2].[Mn+2].[Mn+2].[Mn+2].C1C=CC=CC=1>[C:1]([O:5][C:6]([NH:8][CH2:9][C:10]1[CH:11]=[C:12]([NH:16][C:17]2[C:22]([CH:23]=[O:24])=[CH:21][CH:20]=[C:19]([O:25][CH3:26])[N:18]=2)[CH:13]=[CH:14][CH:15]=1)=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

4

Reactant 1

HCID 18331414HCID 18331414, compound

Product 1

HCID 18331452HCID 18331452, compound

Reagents, catalysts & solvents 2

HCID 131723023HCID 131723023, compoundCatalystHCID 241BenzeneSolvent

Procedure

A mixture of the compound (24 mg) obtained in Example 454, manganese tetraoxide (40 mg) and benzene (8 ml) was stirred at room temperature for 2 days.

Sources & evidence

ORD record
ord-0f6ed2c9695e4baaa54fdb88bd0c0d87
Source dataset
uspto-grants-2001_12
Patent number
US06331553B1

Reaction notes

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