HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 22998514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 2-Butyl-1-benzothiophene | HCID 10655312 | — |
| Product | HCID 22998514 | HCID 22998514 | — |
Reaction Steps
2-n-Butylbenzo[b]thiophene-3-sulfonyl chloride was prepared by the method of Example 40B with DMF (6.6 mmoles, 0.51 ml), sulfuryl chloride (5.6 mmoles, 0.45 ml) and 2-n-butylbenzo[b]thiophene (3.3 mmoles, 0.63 g). Flash chromatography (2% ethyl acetate/hexanes) provided 0.68 9 (71%) of an orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06331637B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-e492efd087704d3aa400e8cda4616bc0 |
| Source note | uspto-grants-2001_12 |