HCID 135767327, compound → HCID 135767342, compound

Participants

Reaction Steps

A mixture of the title compound from example 61 (80 mg, 0.16 mmol) and 10% palladium on charcoal (10 mg) in ethanol (4.5 ml) and water (0.5 ml) was hydrogenated at 60 psi (414 kPa) and 40° C. for 18 hours. The reaction mixture was filtered through Celite®, and the filtrate evaporated under reduced pressure to afford the title compound, (27 mg, 32%).

Provenance & Evidence