HuagongsheHuagongshe Chemistry Print Report · For research reference only
(1-Methylcyclopropyl)methanol → N-[(3-chlorophenyl)acetyl]alanine (1-methylcyclopropyl)methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (1-Methylcyclopropyl)methanol | HCID 137701 | — |
| Reactant | N-(3-chlorophenylacetyl)alanine | HCID 15481783 | — |
| Product | N-[(3-chlorophenyl)acetyl]alanine (1-methylcyclopropyl)methyl ester | HCID 20613258 | — |
Reaction Steps
Following General Procedure C above, and using N-(3-chlorophenylacetyl alanine (from Example D above) and (1-methylcyclopropyl)methanol (Aldrich) the title compound can be prepared. The reaction was monitored by tlc on silica gel and purification was by liquid chromatography using 3:7 EtOAc:hexane as the eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06333351B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-49b8ba9dce3c4ee08d84f496a07fb473 |
| Source note | uspto-grants-2001_12 |