HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → Ethyl 2-(2,4,5-trifluoro-6-methylbenzoyl)-3-ethoxyacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl (3,4,6-Trifluoro-2-methylbenzoyl)acetate | HCID 14517129 | — |
| Reactant | Ethylorthoformate | HCID 53630039 | — |
| Product | Ethyl 2-(2,4,5-trifluoro-6-methylbenzoyl)-3-ethoxyacrylate | HCID 54242925 | 90% |
Reaction Steps
To 3.2 g of ethyl 2-methyl-3,4,6-trifluorobenzoylacetate were added 3.0 g of acetic anhydride and 2.7 g of ethyl orthoformate, followed by heating and refluxing for 1 hour. The resulting mixture was concentrated to give 3.5 g of ethyl 2-(2-methyl-3,4,6-trifluorobenzoyl)-3-ethoxyacrylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06333431B1 |
| Source dataset | uspto-grants-2001_12 |
| ORD ID | ord-f59dd24e8e8b469b9585b26249e1029a |
| Source note | uspto-grants-2001_12 |