Hexane → Undec-2-ene

HRID 2271279Notes

Reaction equation

HRID 2271279 reaction equation
[Cl-].[NH4+].[CH3:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]>>[CH3:3][CH:4]=[CH:5][CH2:6][CH2:7][CH2:8][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Reactant 2

HCID 8058HexaneHCID 25517Ammonium Chloride

Product 1

HCID 34320Undec-2-ene

Procedure

At the end of reaction, 50 ml of a saturated ammonium chloride aqueous solution and 100 ml of n-hexane were added to the reaction solution. The organic layer was extracted, dried over magnesium sulfate, and filtered. By distilling off the solvent, there was obtained 12 grams of 2-undecene in a substantially quantitative yield.

Workup

  1. additionwere added to the reaction solution
  2. extractionThe organic layer was extracted
  3. dry with materialdried over magnesium sulfate
  4. filtrationfiltered
  5. distillationBy distilling off the solvent

Sources & evidence

ORD record
ord-430df3d3eada4e58932f575b67d034cb
Source dataset
uspto-grants-2001_12
Patent number
US06333441B1

Reaction notes

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