2,4-Dimethylaniline → HCID 18419485, compound

HRID 2271296Notes

Reaction equation

HRID 2271296 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][C:3]=1[CH3:9].Cl[C:11]1[CH:16]=[CH:15][C:14]([N+:17]([O-])=O)=[CH:13][N:12]=1.[CH:20]1(N(C2C=CC(N)=CN=2)C)CCCCC1>>[CH3:9][C:3]1[CH:4]=[C:5]([CH3:8])[CH:6]=[CH:7][C:2]=1[N:1]([C:11]1[CH:16]=[CH:15][C:14]([NH2:17])=[CH:13][N:12]=1)[CH3:20]

Participants

4

Reactant 3

HCID 72502,4-DimethylanilineHCID 783082-Chloro-5-nitropyridineHCID 15887620HCID 15887620, compound

Product 1

HCID 18419485HCID 18419485, compound

Procedure

2-(N-(2,4-dimethylphenyl)-N-methylamino)-5-amino-pyridine was prepared from 1-amino-2,4-dimethylbenzene and 2-chloro-5-nitropyridine in the same manner as 2-(N-Cyclohexyl-N-methylamino)-5-amino-pyridine was prepared.

Workup

  1. customwas prepared

Sources & evidence

ORD record
ord-db253db4511f4e65b79059a27892b8ef
Source dataset
uspto-grants-2001_12
Patent number
US06333341B1

Reaction notes

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