Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Propylene Glycol | HCID 1030 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20456454 | HCID 20456454 | — |
Reaction Steps
Activated silica gel of step (1) and tetrahydrofuran are stirred at ambient temperature, then 70 ml of propylene glycol is added (adding 0.2 ml of propylene glycol per gram of silica gel) at ambient temperature, after stirring 1 hour the temperature is raised to 40° C., then mixture of silica gel HHV-4/propylene glycol/THF is obtained;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09120089B2 |
|---|
| Source dataset | uspto-grants-2015_09 |
|---|
| ORD ID | ord-13179653163d48aca8fe88346dfff888 |
|---|
| Source note | uspto-grants-2015_09 |
|---|
